preparation of nitrobenzene pdf

Nitro Benzene preparation, Laboratory & Industrial, Uses and Applications, 77% found this document useful (13 votes), 77% found this document useful, Mark this document as useful, 23% found this document not useful, Mark this document as not useful, Save Nitro Benzene preparation, Laboratory & Industrial... For Later, Benzene exposure has serious health effects. The nitronium ion attacks to the benzene ring resulting in the formation of a carbocation. Process according to claim 2, characterised in that evaporation by concentration takes place in at least five stages. In the process for the preparation of nitrobenzene wherein benzene is reacted with an acid mix consisting essentially of an aqueous mixture of nitric and sulfuric acids, the improved method of refining the crude nitrobenzene obtained from the said reaction which comprises physically separating the crude nitrobenzene from the ReferencesCited in the file of this patent UNITED STATES PATENTS 2,773,911 DubOis et al Dec. 11, 1956. In this way, impairment of the acid evaporation in the evaporator can be excluded. from nat. If 60 to 70% nitric acid (10) is used, it is advisable to evaporate the sulfuric acid to 90 to 93% H. Instead of the environmentally conscious but complex stripping of the vapor condensate, benzene washing to remove the nitrobenzene and biological cleaning of the benzene-containing wastewater are also possible. JOSEF MEISSNER GMBH & CO, Kind code of ref document: 3. In this way, the cost-intensive extractive nitric acid distillation can be replaced by the water evaporation from sulfuric acid according to the invention under optimal conditions. Process for the preparation of nitrobenzene Download PDF Info Publication number EP0156199B1. Designated state(s): In addition to the simple construction and operation, the latter offer the advantage that due to the multi-stage water evaporation mainly takes place at such low sulfuric acid concentrations that even evaporation to an H. The embodiment of the method according to the invention is particularly preferred, in which the evaporation is carried out in one or more interconnected horizontal evaporators. 3,928,475; US Pat. Process according to one of the claims 1 to 4, characterised in that the diluted sulphuric acid is heated by the acid which has been concentrated. 39,556; US Pat. 7. Alternatively, the nitro bodies can be extracted with the benzene used for the production of nitrobenzene and the vapor condensate containing benzene can be sent to a wastewater treatment. No. The vapor condensation can alternatively take place by direct contact of the vapor with vapor condensate, which is conveyed in the circuit via a cooler. Application filed by EI Du Pont de Nemours and Co, 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EIDU PONT NEMOURS AND COMPANY Wilmington US, 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Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton, Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups, Process for refining aqueous acid mixtures utilized in nitration of aromatics, Nitric acid recovery by the adiabatic nitration of nitroaromatics with fortified spent acid, Process for separating nitroaromatic compounds from spent nitric acid, Recovery of nitric acid from nitration spent acid by toluene extraction, Conitration of mixed aromatic hydrocarbons, Process for preparing mixtures of diphenyl-methane diisocyanates and polyphenyl-polymethylene polyisocyanates, Process for preparing polyisocyanates from biomass, Adiabatic process for nitration of nitratable aromatic compounds, Process for working up the waste water obtained in the preparation of dinitrotoluene, Process for obtaining gaseous hydrogen chloride from dilute, aqueous hydrochloric acid, Production of dicarboxylic acid anhydrides, Removal of acidic gases from hydrocarbon streams, Production of hydrogen fluoride and metal sulfates, Process for working up secondary components in the preparation of dinitrotoluene, Process for the preparation of mononitro-aromatic compounds, Method and apparatus for purifying nitration products, Continuous process for the production of peroxycarboxylic acid compositions, Improvements in or relating to the production of solid non-ionic surface active agents, Process for purification of polytetramethyleneether, Nitric acid recovery from nitriding processes, Process for the production of dinitrotoluene, Single-stage process for the preparation of terephthalic acid, Method for nitration of aromatic hydrocarbon compounds, A process for the manufacture of nitric acid esters, Process for the two-step production of dinitrotoluene.